简介：Let'stakeHasaninfinite–dimensionalHilbertspaceandK(H)bethesetofallcompactoperatorsonH.UsingSpectraltheoremforcompactself–adjointoperators,weprovetheHyers–UlamstabilityofJensen*-derivationsfromK(H)intoK(H).

简介：Weestablishseveralfundamentalidentities,includingrecurrencerelations,degreeelevationformulas,partitionofunityandMarsdenidentity,forquantumBernsteinbasesandquantumBeziercurves.WealsodeveloptwotermrecurrencerelationsforquantumBernsteinbasesandrecursiveevaluationalgorithmsforquantumBeziercurves.Ourproofsusestandardmathematicalinductionandotherelementarytechniques.

简介：选用aug-cc-pVTZ及aug-cc-pVQZ基组对不同H2-H2位形进行了量子化学计算,外推出了氢分子间各向异性ab-initio作用势。依据实验数据确定出氢分子相互作用的5-体模型,在全局最优算法基础上拟合出了包含电四极矩项、多体极化作用项及三体关联项等在内的氢分子间各向异性作用势。结果验证了拟合势与ab-initio势能曲线几乎重合,两者偏差落在（-1.35K,1.29K）范围内;得出的氢分子第二维里系数与实验结果一致。

简介：对化合物[Na_2（H_2O）_（10）][Cu_4（H_2O）_（12）（H_2W_（12）O_（42））]·15H_2O（简称Na_2Cu_4W_（12））进行了体外抗肿瘤活性研究.应用四甲基偶氮唑盐（3-[4,5-dimethylthiazo-2-y]-2,5-diphenyltetrazoliumbromide,MTT）比色法分析Na_2Cu_4W_（12）对人肝癌细胞（HepG2）、人神经母细胞瘤细胞（SHY5Y）增殖抑制活性.采用光学显微镜观察肿瘤细胞的凋亡形态变化,用流式细胞术分析细胞周期和细胞凋亡,计算各期细胞比例及细胞凋亡率.结果表明,Na_2Cu_4W_（12）对HepG2和SHY5Y2种肿瘤细胞增殖半数抑制浓度IC_（50）值分别为5.3和10.2μmol·L~（-1）,且呈剂量依赖性.光学显微镜下处理组细胞出现皱缩、变圆、缩小等形态变化,不同浓度Na_2Cu_4W_（12）处理12h早期凋亡细胞所占的百分比显著增加且呈剂量依赖性.综上所述,Na_2Cu_4W_（12）能够抑制胞瘤细胞增殖,诱导细胞凋亡.

简介：Themainworkoftheirradiationtechniquegroupfocusesonthefollowingtwoaspectsin2016:1.TechniquesupportWehavehadabout772.5hbeamtimefor39roundsofsingleeventeffect(SEE)tests,whichiscooperatingwithvariousinstitutes,universities,andcompanies.Thetestsarethebasicsafeguardforthespacecraftandsatellite.InordertoguaranteethetestefficiencyoftheTerminal5,themaintenanceandimprovementforthevacuum,thesampletransferandbeammonitorsystemhavebeenachieved.

简介：在未采取预电离措施的情况下，研究了纯sf6气体及sf6/h29sf6/c2h6两种混合气体激光介质脉冲放电特性。实验结果表明，无预电离时SF68其混合气体介质可以实现自引发体放电，气体介质体放电维持电压主要由SF,;含量决定，C2H6具有抑制电弧的作用，可以有效延长体放电维持时间。分析认为，sf66体高折合场强E/P导致的放电通道电流密度受限和高电负度■引起的放电通道中负离子分解产生二次电子，是介质实现自引发体放电的重要机理。

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简介：Takingadvantageofthelargeγ-detectorarrayGammasphereandtherecoilmassseparatorFMA,highspinstatesin117Bawereinvestigatedthroughtherecoil-β-delayedprotondecaytaggingtechniqueviatheheavy-ioninducedfusion-evaporationreaction64Zn(58Ni,2p3n)117Ba,atabeamenergyof305MeV.Promptγraysbelongingto117Bahavebeenidentifiedfurthermore,arotationalbandhasbeenidentifiedforthefirsttimeandpresentedasbandAinFig.1.

简介：Twofamiliesofcatalysts,basedonPdnanoparticlessupportedonceramicasymmetrictubularaluminamembranes,arestudiesinthedirectsynthesisofH_2O_2.TheyarepreparedbydepositingPdintwoways:(i)reductionwithN_2H_4inanultrasonicbathand(ii)byimpregnation-deposition.Thefirstpreparationleadstolargerparticles,withaveragesizeofaround11nm,whilethesecondpreparationleadstosmallerparticles,withaveragesizearound4nm.Thecatalyticmembranesweretestedasprepared,afterthermaltreatmentinairandafterfurtherpre-reductionwithH_2inmild(100℃)conditions.SampleswerecharacterizedbyTEM,CO-chemisorptionmonitoredbyDRIFTSmethodandTPR,whilecatalytictestshavebeenperformedinasemi-batchrecirculationmembranereactor.Experimentalcatalyticresultswereanalysedusingtwokineticsmodelstoderivethereactionconstantsfortheparallelandconsecutivereactionsofthekineticnetwork.SmallerparticlesofPdshowlowerselectivityduetothehigherrateofparallelcombustion,evenifthebetterdispersionofPdandthushighermetalsurfaceareainthesampleleadtoaproductivityinH_2O_2similarorevenhigherthanthesamplewiththelargerPdparticles.IndependentlyonthepresenceofsmallerorlargerPdnanoparticles,anoxidationtreatmentleadstoasignificantenhancementintheproductivity,althoughthecatalystprogressivelyreducesduringthecatalyticprocess.Theinhibitionoftheparallelcombustionreaction(towater)inducedfromthecalcinationtreatmentremainsafterthein-situreductionoftheoxidizedPdspeciesformedduringthepre-treatment.Thisislikelyduetotheeliminationofdefectsiteswhichdissociativelyactivateoxygen,andtentativelyattributedtoPdsitesabletogivethree-andfour-foldcoordinationofCO.

简介：WereportontheobservationofsubcycleinterferencesofelectronwavepacketsreleasedduringstrongfieldionizationofH2withcycle-shapedtwo-colorlaserfields.Withareactionmicroscopewemeasurethree-dimensionalmomentumdistributionsofphotoelectronscorrelatedwitheitherH2+orprotonswithindifferentenergyrangesgeneratedbydissociationofH2+.Werefertothesedifferenttypesofphotoelectronsaschannels.Ourresultsshowthatthesubcycleinterferencestructuresofelectronwavepacketsareverysensitivetothecycleshapeofthetwo-colorlaserfield.Weexplainthisbehaviorbythedependenceoftheionizationtimewithinanopticalcycleontheshapeofthelaserfieldcycle.Thesubcycleinterferencestructurescanbefurtherusedtoobtaininsightintothesubcycledynamicsofmoleculesduringstrongfieldinteraction.

简介：Inthispaper,weinvestigatetheglobalexistenceandlongtimebehaviorofstrongsolutionsforcompressiblenematicliquidcrystalflowsinthreedimensionalwholespace.TheglobalexistenceofstrongsolutionsisobtainedbythestandardenergymethodundertheconditionthattheinitialdataareclosetotheconstantequilibriumstateinH~2-framework.IftheinitialdatasinL~1-normarefiniteadditionally,theoptimaltimedecayratesofstrongsolutionsareestablished.WiththehelpofFouriersplittingmethod,onealsoestablishesoptimaltimedecayratesforthehigherorderspatialderivativesofdirector.

简介：本文的主要工作有：分析了国内外杨氏模量测量的原理与方法;把测量装置由悬挂法改为支撑法,增加了实验棒的长度（原实验棒长度16cm,新实验棒长度23cm）,扩大了数据的测量范围;移动支架置于导轨上,可直接在导轨标尺上准确读数,每隔3mm测一次数据,数据增多;组装调试实验装置,测量了黄铜、纯铜、钛三种材料的杨氏模量并进行数据处理,将改进后实验系统测得的结果和原实验系统测得的结果以公认值进行比较,完善了改进后实验系统的教学功能.

简介：根据相关监督检查制度及备案通知要求，临沂市在全市25家代理记账机构进行自查的基础上，于6月12日-23日对三个县区的10家代理记账机构进行了重点检查。检查项目多。本次检查除对经营场所、会计人员情况、制度建设、会计核算业务进行检查外，同时对代理记账机构财经纪律遵守情况及自身会计工作质量进行了监督检查。

简介：AseriesofnovelN-（3-furan-2-yl-1-phenyl-1H-pyrazol-5-yl）amidesderivativesweredesignedandsynthesized.Theirstructureswereconfirmedby1HNMR,13CNMRandHRMS.Alltitlecompoundswereevaluatedfortheirherbicidalandantifungalactivities.Preliminarybioassayresultsindicatedthatthetitlecompoundsshowedgoodtomoderateherbicidalactivityat1000mg/L.Compound6qpresentedthebestactivityagainstDigitariasanguinalis（L）Scop.,AmaranthusretroflexusL.andArabidopsisthalianawithaninhibitiondegreeoffive.Compound6dalsoshowedaninhibitiondegreeoffiveagainstD.sanguinalis.Inaddition,at50mg/L,mostcompoundsexhibitedgoodinvitroantifungalactivityagainstSclerotiniasclerotiorum,withcompound6cshowingover90%antifungalactivityagainstS.sclerotiorumandPelliculariasasakii.

简介：本文使用函数性数据分析方法中相平面图技术，考察中国三大行业及其子行业并购重组动态路径演变，同时探索国家行业政策和经济金融环境的变化对并购动态演变的影响．本文发现随着产业经济规模的发展，整个并购重组频次呈现上升趋势；第一产业的动态演变路径呈现出低一高一低的“收缩螺旋”特征，第二、三产业的发展呈现出低一高一低一高的“扩张螺旋”动态演变路径；股权分置改革、金融危机、行业政策的出台等事件严重影响相关产业的并购重组动态演变路径．

简介：TostudytheintramolecularDiels-Aldercycloadditonof2H-chromen-2-oneasadiene,aseriesofchiralN-allyl-N-benzylamidesthatcontaina2H-chromen-2-onemoietyweredesignedforthesynthesisofbenzo[f]isoindol-l-onesviaanintramolecularDiels-Alderandasubsequentretro-Diels-AldercycloadditionwiththeexpulsionofCO2.Boththeyield（80%-89%）andabsolutestereocontrolofthetandemreactionwerehighwhenanelectron-withdrawinggroupwasattachedtothedienophile.Thedoublebondinthestyrenesubstructureremainedintheproductscouldbefurtherderivatizedbydihydroxylation.

简介：以4-[（8-羟基-5-喹啉）偶氮]-苯磺酸与氯化钴为原料,采用溶剂热法通过原位反应合成{[Co（5-氨基-8-羟基喹啉）_2]·H_2O}_n,并通过X-射线单晶衍射方法确定了该配合物的晶体结构.结构分析表明：标题配合物属于斜方晶系,Pbcn空间群,晶胞参数a=1.321（2）nm,b=0.811（2）nm,c=1.511（2）nm,α=β=γ=90.00°,V=1.619（3）nm~3,Z=4,R_1=0.0516,wR_2=0.1025.配合物中存在ππ堆积相互作用和氢键作用,将配合物连接形成三维超分子网络结构.

简介：网格生成技术是CFD复杂工程应用的重要环节，网格质量的好坏直接影响计算结果的精准度，因此其已成为CFD的重要研究领域．在张涵信院士的指导下，作者自20世纪90年代初开始开展非结构网格、混合网格技术和相应的计算方法研究，并逐步发展至动态混合网格技术及非定常计算方法．在张涵信院士80华诞之际，对近年来作者及团队在网格生成技术及应用方面所取得的进展进行了简要的综述，分别介绍了静动态混合网格生成、定常／非定常计算方法、网格技术的应用等方面的进展情况．最后，就网格生成技术目前还存在的问题．展望了未来的发展方向．作者谨以此文表达对张涵信院士25年来的培养、关怀和帮助的崇高敬意．

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简介：采用普通溶液法合成了锰配位聚合物[Mn（C_（10）H_8N_2）（CHO_2）_2]_n,并用红外光谱、紫外光谱、X-射线单晶衍射、热重分析和电化学分析对其进行表征.晶体结构表明：该配合物属于单斜晶系,Pn空间群,晶胞参数a=0.7828（6）nm,b=0.8650（6）nm,c=0.9021（7）nm,β=90.304（7）°,V=0.6108（8）nm3,Z=1.Mn（Ⅱ）离子的配位多面体呈变形的八面体几何结构.配合物由配体甲酸根离子和4,4＇-联吡啶桥联为三维网状结构.