学科分类
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21 个结果
  • 简介:ItisfundamentallyimportanttounderstandtheinfluenceofstrainonthedensityofdeformationtwinsinTWIPsteelbecausetwinningisitsdominantdeformationmechanism.ThedeformationbehaviorofaFe-30Mn-4Si-3Al-0.097CsteelhasbeeninvestigatedbyX-raydiffraction(XRD),electronbackscatterdiffraction(EBSD)andtransmissionelectronmicroscopy(TEM)techniques.Samplewithanaveragegrainsizeof10μmwasdeformedincold-rollingwithareductionof10%,20%,30%,40%,50%,60%and70%,respectively.Themechanicalpropertiesofthecold-rolledsampleswerefurtherinvestigatedbytensiletests.Theyieldstrength(σy)andultimate-tensile-strength(σUTS)oftheas-preparedsampleis480MPaand850MPa,respectively.However,undercoldrollingdeformation,thetensilestrengthobviouslyincreaseswithanincreaseinrollingreduction.Thesamplewitharollingreductionof10%exhibitsσyof610MPaandσUTSof-1000MPa.Theyieldstrengthandtensilestrengtharefurtherenhancedupto1320MPaand1378MPaforthespecimenwitharollingreductionof70%,regardlessofthepoorductilityof6.7%.ThedeformationmicrostructureswerestudiedbyEBSDandTEMobservations.Itisfoundthat,withincreasingrollingreduction,theaveragedistancebetweendeformationtwinsdecreasesgraduallywhilethedensityofdeformationtwins(thelengthoftwinboundaryinunitarea)exhibitamaximumvalueat40%cold-rolling+tension.Carefullystatisticsanalysisrevealsgrainorientationiscloselyrelatedtothedeformationtwinsandtheunderlyingmechanismgoverningthetwinningisdiscussed.

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  • 简介:Thestudyintroducesthechemicalcomposition,mechanicalproperties,physicalpropertiesandproductionprocessesoftheFe-23Mn-2Al-Vausteniticsteel.Investigationsweremadeintotheformationofcracksinthehot-rolledFe-23Mn-2Al-Vsteelplates,withopticalmicroscopy(OM),scanningelectronmicroscopy(SEM)andenergydispersivespectrum(EDS).Theresultshaveshownthatintergranularoxidationinthereheatingfurnaceisthemaincauseofthecracksonthesurfaceofthehot-rolledsteelplates.Thesurfacecrackingcanbelargelyavoidedbycontrollingtheremainingoxygencontentinthereheatingfurnaceandimprovingcontinuouscasting(CC)processestoincreasethethicknessoffineequiaxedgrainlayerofthesteelslabs.

  • 标签: 奥氏体不锈钢 表面裂纹 热轧板 扫描电子显微镜 Fe 热轧钢板
  • 简介:铁矿石经浓盐酸和少量的SnCl2溶液加热到45℃溶解后,用SnCl2-TiCl3还原滴定Fe(Ⅲ),使Fe(Ⅲ)还原为Fe(Ⅱ),再以K2Cr2O7滴定全铁含量。本方法对实验操作温度,试样溶解酸的选择有一定的要求,宜选用非氧化性强酸在30-60℃溶解矿样。

  • 标签: 铁矿石 SnCl2-TiCl3-K2Cr2O7滴定法 Fe(Ⅱ) Fe(Ⅲ)
  • 简介:采用碱熔处理样品,酸化后,移取部分溶液稀释后引入ICP测定ZrO2、TiO2、Fe2O3含量,剩余溶液用强碱分离钛、铁、锰等干扰元素后,EDTA—CuSO4法返滴定Al2O3,终点明显,检测重现性好;

  • 标签: FE2O3 AL2O3 ZRO2 TIO2 测定方法 质砖
  • 简介:近来,钢板市场对建筑屋顶和外墙等功能性薄板需求在不断增大。JFE公司的镀锌和涂层产品已用于各种建筑以满足节能、防菌、防霉、防静电和抗热等性能的需求,JFE镀锌和涂层公司生产了各种涂层钢板。除了优秀的防菌和防霉产品PURE—CLEAN之外,还有能很好防止静电的CLEAN—ACE产品以及耐热产品BAKE—CLEAN。

  • 标签: 涂层钢板 节能建筑 CLEAN 涂层产品 建筑屋顶 PURE
  • 简介:1前言在电炉炼钢生产过程中,使用涂层吹氧管代替非涂层吹氧管进行吹氧操作,可以减少吹氧管消耗、降低炼钢生产成本,提高经济效益,此项措施已在许多电炉钢厂广泛采用。鉴于此,我们分别于1993年上半年及1994年上半年在一炼钢厂和二炼钢厂采用涟钢振兴冶金材料厂生产的涂层吹氧管进行了试验,考察了涂层吹氧管的使用效果,现已全面推广使用,效果良好。

  • 标签: 吹氧管 表面涂层 炼钢厂 电炉炼钢 涂层管 推广使用
  • 简介:Cr2O3-formingferriticstainlesssteelshavebeenwidelyexploredasintermediatetemperaturesolidoxidefuelcells(SOFCs)interconnects.However,theevaporationofchromiascalemightmigratetoandpoisonthecathode,leadingtodegradationofthecellperformance.Inthisstudy,Ni-Co-Fe-Pcoatingsweredepositedontheferriticstainlesssteelbymeansofacost-effectivetechniqueofelectrolessmethod.Theyareexpectedtobeconvertedinto(Ni,Co,Fe)3O4spinelwithahighelectricalconductivityandCTEmatchwithstainlesssteel,whichcanblocktheevaporationofchromiaformedonsteelsubstrateexposedtothecathodeenvironmentoftheSOFC.TheeffectsofpH,massratioofFeSO4/(FeSO4+NiSO4+CoSO4)andtemperatureofsolutiononthedepositionrate,compositions,surfacemorphologiesandstructuresoftheNi-Co-Fe-Pcoatingswereinvestigated.TheresultsindicatedthatthedepositionrateincreasedwithincreasingpHwhenpHwaslowerthan9andthenreducedwhenpHwashigherthan9.Thedepositionrateincreasedwithincreasingtemperaturewhentemperaturewaslowerthan80℃andthendecreasedwhentemperaturewashigherthan80℃.ThedepositionratedecreasedwiththeincreaseinmassratioofFeSO4/(NiSO4+CoSO4+FeSO4).ThecoatingsconsistedofNi,Co,FeandP.Thephasestructureofthecoatingwasamorphous.

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  • 简介:ThehotductilityofFe-36NiinvaralloywithdifferentadditionsoftheelementceriumwasinvestigatedusingaGleeble-3800thermal-mechanicalsimulatoroverthetemperaturerange850-1050℃,andtheimprovementmechanismofthehotductilitywasanalyzedusingacombinationofSEM,EDS,andOM.TheresultsindicatedthatFe-36Niinvaralloyexhibitedpoorhotductilitybelow1050℃,whichwasmainlyattributedtoweakgrainboundariesandtheactionofgrainboundarysliding.However,thealloyswithceriumcontentsof0.016%and0.024%bothdemonstratedsubstantialimprovementinthehotductilityovertheentiretestingtemperaturerange.Theobservedimprovementofthehotductilityofthealloywith0.016%ceriumat950℃andthealloywith0.024%ceriumat900℃wasassociatedmainlywiththegrainboundarystrengtheningandtherestrictionofthegrainboundaryslidingbecausetheadditionofceriumreducedthesegregationofsulfuratgrainboundariesandrefinedthegrainstructure.Theoccurrenceandaccelerationofdynamicrecrystallizationwerefoundtoberesponsibleforthehighhotductilityofthealloywith0.016%ceriumat1000℃andthealloywith0.024%ceriumat950-1000℃asaresultoftherefinementofthegrainstructurebyadditionofcerium.

  • 标签: 因瓦合金 高温塑性 晶界滑移 温度范围 晶粒结构
  • 简介:TheeffectofCe,LaandmischmetalonthesolidificationstructureofFe-36Niinvaralloywasinvestigated.Theresultsshowthatgreatamountsofhigh-meltingpointcompounds(Ce2O3,La2O2Sand(Ce,La)2O2S)respectivelyformedinthealloywiththeadditionofCe,Laormischmetal.Basedonthetheoryoflatticemisfit,thelatticemisfitbetweenthe(0001)surfacesofCe2O3,Ce2O2SandLa2O2Sand(100)surfaceofFe-36Niinvaralloywere6.21%,5.77%and5.42%,respectively,whicharerelativelylow.Therefore,Ce2O3,La2O2Sand(Ce,La)2O2Scouldserveasthecoreofheterogeneousnucleation,improvetheequiaxedgrainratio,reducetheequiaxedgrainsizeandrefinethesolidificationstructureofalloy.

  • 标签: 因瓦合金 混合稀土 凝固组织 非均质形核核心 催化能力 晶格失配
  • 简介:碳钢薄板厂转炉一次除尘采用湿式法除尘,存在以下问题:1、转炉烟气中的灰尘、水汽和混合气体在风机作用下,形成高速气流,严重冲刷、侵蚀风机转子前后端板、叶片。2、转炉烟气中的灰尘附着在转子前盘、后盘和叶片表面,破坏转子动平衡,转子使用周期较短。"3、影响风机轴瓦、偶合器使用寿命,对风机基础也产生较大影响。4、转子在线使用周期短,检修时间长,人力物力消耗巨大,不利于设备管理和降低费用消耗。炼钢保障作业区相关技术人员针对转炉一次除尘风机转子工作特点和工作环境,进行了多方面分析、论证,在转子表面喷涂金属保护层、对转子反冲洗系统进行改进,降低了转子振动,延长了转子使用周期,缩短了检修时间和人力物力财力消耗,避免了转炉烟气中烟尘、水分及腐蚀性气体对转子及叶片表面的冲刷和侵蚀,延长转子使用寿命,提升了设备综合效益。

  • 标签: 风机转子 涂层 动平衡 反冲洗水
  • 简介:Inthepresentstudy,sampleswereextensivelycollectedthroughoutthestainlesssteelmanufacturingprocess.Thethree-dimensionalmorphologyofinclusionswasrevealedbynon-aqueoussolutionelectrolysis.Thehighconcentrationofaluminuminferrosiliconcausedtheincrementof[Al]sinsteelandAl2O3ininclusions,whichledtothehighermeltingtemperatureofinclusions.ItwasconcludedthattheapplicationoflowAlferrosiliconandcalciumtreatmentcouldpreventtheformationofAl2O3-richinclusions.

  • 标签: 奥氏体不锈钢 夹杂物控制 O3 低铝硅铁 水溶液电解 制造过程
  • 简介:Thehot-deformationbehaviorofFe-Mn-Ctwinninginducedplasticity(TWIP)steelwasinvestigatedbyconductinghotcompressiontestswithinarecommendedhotrollingtemperaturerangeatvariousstrainrates.Flowresistancecurvesduringhot-deformationwereobtained,andstrainratesensitivitiesandactivationenergiesforplasticdeformationwerecalculatedusingthepowerlaw.ItisfoundthattheadditionofAlandSiclearlyincreasesthepeakstressesforthepresentalloys,especiallyat950℃.ButMnhasaminoreffectonthestress-straincurvesandactivationenergywhenitscontentvariesfrom15mass%to22mass%forthepresentalloys.

  • 标签: 炼钢过程 温度范围 热轧 冶炼技术
  • 简介:AluminumfilmscoatedonDIsteelsheetswerepreparedbydirectcurrent(DC)magnetronsputtering.Theinfluenceofthedepositionconditionsandfilmthicknessontheformabilityofcoatedsteelsheetswasstudied.TheresultsofthecuppingtestanddrawingtestshowthatthesubstratetemperatureandthicknessofAlfilmsarethekeyfactorsthataffectAladhesionandformabilityofcoatedsteelsheets.AdhesionbecameworsewhenthethicknessofAlsheetswasmorethan2μm.Andformabilitywasimprovedremarkablywhenthesubstratetemperaturewasincreasedto200℃.

  • 标签: 涂层钢板 磁控溅射 溅射制备 铝薄膜 机械性能 DI
  • 简介:Resultspresentedinthisstudycontributetoinvestigationofthemicrostructureandmechanicalpropertiesofthehot-rolledFe16Mn0.6Csteelplates.Thesteelplateshavebeenproducedbybeinghot-rolledattemperaturesrangingfrom1100℃to850℃insevenpassesto97.5%reductioninthicknessandthencooledinafurnaceof650℃.Someplateshavebeenannealedattemperaturesrangingfrom300℃to1100℃for5minto60min,andthenfollowedbywaterquenching.Thereareannealingtwinsinthehot-rolledFe16M...

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  • 简介:TheFe-Ti-Nmateralloywaspreparedthroughthein-situreactionofnitrogengaswiththeFe-Timelt.ScanningelectronmicroscoperesultsshowthattheparticlesuniformlydistributedintheironmatrixwereTiN.ThedeliberatelypreparedFe-Ti-Nmasteralloywasemployedforthe409Lferriticstainlesssteelinanattempttorefinetheas-castsolidificationstructure.ItwasfoundthattheeffectivenessofFe-Ti-Nmasteralloyonrefiningoftheas-cast409Lferriticstainlesssteelwasaffectedbyadditionlevel,holdingtimeandmeltstemperature.Itwasfoundthattheaverageequiaxedgrainsizedecreasedfrom1503μmto303μm,theproportionofequiaxedgrainzoneincreasedfrom14%to100%withincreasingtheFe-Ti-Nmasteralloyadditionlevelto2.5%.Theproportionofequiaxedgraindecreasedfrom85%to4%asthesolidificationtemperatureincreasedfrom1803Kto1883K.Whentheholdingtimereachedto8min,thesolidificationstructuresof409Lferriticstainlesssteelshowextremepointsintheproportionofequiaxedgrain.Itisclearthatthegrainrefiningefficiencygraduallyfadeawaywiththeincreasingoftheholdingtimeattheverybeginning.However,whentheholdingtimecontinuestoincreaseandexceedstheextremepoint,thegrainrefiningefficiencyoftheFe-Ti-Nmasteralloyrecoveredtoacertaindegree.Theexperimentalresultsmentionedabovehavebeenanalyzedintermsofthermodynamics.Underappropriateconditions,theFe-Ti-Nmasteralloyusedforgrainrefinementofthesolidificationstructureof409Lferriticstainlesssteelmayhavegoodprospectsforindustrialapplications.

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  • 简介:ThemicrostructuralchangesofFe83Si4B13amorphousmotheralloyduringtheheatingprocesswereinvestigatedbyLaserScanningConfocalMicroscopy(LSCM),andthephasetransformationwasdeterminedbytheThermo-Calccalculations.ThedifferencesinthemeltingpointsmeasuredbyDifferentialScanningCalorimetry(DSC)andLSCM,andthoseobtainedbyThermo-Calccalculationswerealsodiscussed.ItisfoundthatthemeltingpointsmeasuredbyDSCandLSCMarerelativelysimilar,whereastheonsetandendofthemeltingtemperaturescalculatedbyThermo-CalcsoftwarearehigherthanthosemeasuredbyDSCandobservedbyLSCM.

  • 标签: 加热过程 计算值 母合金 激光扫描共聚焦显微镜 差示扫描量热法 LSCM
  • 简介:ToimprovethemechanicalpropertiesofWC-Al2O3composites,theeffectsoftraceamountofCeO2additivesonthemicrostructureandmechanicalpropertiesoftheWC-Al2O3compositespreparedbyhotpressingwereinvestigated.TheresultsrevealedthattheWC-Al2O3compositesdopedwith0.1%CeO2possessedrefinedmicrostructureandenhancedmechanicalpropertiescomparedwiththatoftheundopedWC-Al2O3composites.TraceCeO2suppressedthedecarburizationofWC,promotedthemicrostructuralrefinement,andimprovedtheinterfacecoherenceoftheWCmatrixandAl2O3.When0.1%CeO2wasaddedtotheWC-Al2O3composites,theeffectofCeO2resultedintheachievementofarelativedensityof98.82%withanexcellentVickershardnessof16.89GPa,combiningafracturetoughnessof9.85MPa·m1/2withanacceptableflexuralstrengthof1024.05MPa.

  • 标签: 复合材料 力学性能 显微组织 CEO2 添加剂 组织细化
  • 简介:研究不同碳源下Al2O3-SiC-C铁钩料的性能。分别以球沥青、焦炭和炭黑为碳源,比较了常温下三者的显气孔率、抗折和抗压强度。结果表明,不同种类碳源将对试样的气孔率和抗折强度产生不同程度的影响。

  • 标签: 碳源 AL2O3-SIC-C 铁钩料
  • 简介:Opticalmicroscope(OM),scanningelectronmicroscope(SEM),energydispersivespectrometer(EDS)andX-rayDiffraction(XRD)wereusedtostudytheeffectsofrareearthonthemicrostructuralcharacteristicsof55%Al-Zn-1.6%Sihot-dipcoatingsonsteel.TheresultsofOM,SEMandEDSshowedthatbyaddingREintothe55%Al-Zn-1.6%Sibath,thesaw-toothedshapeofintermetallicreactionlayerofcoatingbecamesmooth,andthethicknessoftheoverlayandintermetallicreactionlayerdecreased.TheXRDresultsrevealedthattheintermetallicreactionlayerwascomprisedoftwodifferentregions,abrightphaseclosesttothesteelsubstratewithphasesofFe2Al3andadarkphaseclosesttothemetalliccoatingwithphasesofFeAl3/α-Fe-Al-Si.

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  • 简介:通过改进耐火材料及辅料中Al2O3含量的分析方法,解决了传统分析方法存在滴定终点判断不准、低含量Al2O3分析准确性差的缺点。经大量试验数据证明,改进后的方法可以替代传统分析方法。

  • 标签: AL2O3 熔融 滴定