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A chiral stationary phase with special hydrophobic framework for ligand-exchange chromatography

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摘要新奇chiral为ligand交换层析(CLEC)的静止阶段(CSP1)被第一把dimethylchlorosilane用作在硅石胶化的表面上为减少的剩余silanol组盖住试剂的结束准备，然后同时作为一个chiral选购者和恐水病的辛基组把l职业人员介绍给硅石胶化表面。CSP1上的14dl氨基的酸的enantioseparations被完成，enantioselectivity和在0.8和6.3之间的决定R从1.09～2.44。有用参考方法准备的结合的阶段(CSP2)的CSP1的色析法的表演被比较。结果证明chiral的列效率和决定R静止阶段能被使用上述修改方法改进。

DOI 3j7m7qlvj1/558329

作者 Hong Yu Shi;Rui Juan Song;YU Fu;Na Yao;Yuan De Long;Tian Bao Huang

机构地区不详

出处《中国化学快报：英文版》 2007年11期

关键词氨酰基酯配体交换色谱法手征性光学异构现象

分类 [理学][化学]

出版日期 2007年11月21日（中国期刊网平台首次上网日期，不代表论文的发表时间）

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来源期刊

中国化学快报：英文版

中国化学快报：英文版

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相关关键词

氨酰基酯配体交换色谱法手征性光学异构现象

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