简介:Aliquidmodifiedphotoniccrystalfiber(PCF)integratedwithanembeddeddirectionalcouplerandmulti-modeinterferometerisfabricatedbyinfiltratingthreeadjacentairholesoftheinnermostlayerwithstandard1.48refractiveindexliquids.Therefractiveindexofthefilledliquidishigherthanthatofbackgroundsilica,whichcannotonlysupportthetransmittingrodmodesbutalsothe'liquidmodifiedcore'modespropagatingbetweenthePCFcoreandtheliquidrods.Hence,thelightpropagatingintheliquidmodifiedcorecanbeefficientlycoupledintothesatellitewaveguidesunderthephase-matchingconditions,resultinginadramaticdecreaseoftheresonantwavelengthintensity.Furthermore,thereisamulti-modeinterferenceproducedbymodifiedcoremodesandrodmodes.Suchacompact(~0.91cm)deviceintegratedwithanembeddedcouplerandinterferometerisdemonstratedforhigh-sensitivitysimultaneoustemperature(~14.72nm∕℃)andstrain(~13.01pm∕με)measurement.
简介:Alloymaterialshaveattractedincreasingattentionsbecausetheypossesssuperiorelectricalconductivitywhichcancontributetoexcellentelectrochemicalperformance.HereinadendriticNi3Calloymaterialhasbeenpreparedbythepyrolysisofnickelacetylacetonateemployingoleylamineasareductantand1-octadeceneoroctadecaneasthesolvent.Thecurrent–voltagecurvesindicatingthattheelectricalconductivityofNi3Cishigherthanthatofnickeloxide.Electrochemicaltestingindicatesthatahighspecificcapacityof390C/gisfoundinalkalineelectrolyteat0.5A/g,anddeliverexcellentratecharacteristicaswellascyclelife.Theexcellentelectrochemicalperformancemaybeattributedtoitshighelectricalconductivityanddendriticnanostructurethatcanpromotediffusionofelectrolyteions.Inaddition,theAC//Ni3Casymmetricsupercapacitorhasbeenassembledatacellvoltagesbetween0and1.6V,achievingamaximumenergydensityof37Wh/kg(atapowerdensityof0.3995kW/kg),andthismanifeststhattheNi3Calloyisapromisingelectrodematerialforelectrochemicalenergystorage.
简介:Thispaperhadinvestigatedtheeffectsofsurfacewettabilityonthefrictionalresistanceofturbulenthorizontalflowfortapwaterinfivepipesmadeofvariousmaterialsandfourkindsofliquidsinapolytetrafluoroethylene(PTFE)pipe,withthesameinnerdiameterof14mm.Pressuredropsweremeasuredunderdifferentflowratesthroughanexperimentalflowloop.Thecontactanglesandadhesionworkofliquidsincontactwithpipesurfacesweredeterminedusingacontactanglemeter.Basedonthedimensionandregressionanalyses,twokindsofmodifiedrelationshipsbetweenthefrictionalcoefficientandthesurfacewettabilitywereestablishedaccordingtothemeasuredresultscorrespondingtotapwaterinfivepipesandfourliquidsinPTFEpipe.Theexperimentalresultsshowthatthesurfacewettabilityhassomeinfluenceonfrictionalcoefficientofthestudiedliquidsflowinginmacroscalepipes,andthefrictionalcoefficientdecreaseswiththeincreaseofthecontactangleatthesameReynoldsnumber.Meanwhiletheeffectofwettabilityonthehydrophobicsurfaceisgreaterthanthatonthehydrophilicone.Thefrictionalcoefficientspredictedbythemodifiedformulashaveverifiedtobeingoodagreementwiththeexperimentalvalues,therelativeerrorsofwhicharewithin±6%and±3%forthetapwaterflowinginfivedifferentpipesandfourkindsofliquidsflowinginPTFEpipe,respectively.
简介:Inthisstudy,atwo-stepheatingprocessisintroducedfortransientliquidphase(TLP)diffusionbondingforsoundjointswithT91heatresistantsteels.Atfirst,ashort-timehighertemperatureheatingstepisaddressedtomelttheinterlayer,followedbythesecondsteptocompleteisothermalsolidificationatalowtemperature.Themostcriticalfeatureofournewmethodisproducinganon-planarinterfaceattheT91heatresistantsteelsjoint.WeproposeatransitionalliquidphasebondingofT91heatresistantsteelsbythisapproach.Sincejointmicrostructureshavebeenstudied,wetestedthetensilestrengthtoassessjointmechanicalproperty.Theresultindicatesthatthesolidifiedbondmaycontainaprimarysolid-solution,similarcompositiontotheparentmetalandfreefromprecipitates.Jointtensilestrengthofthejointisnotlowerthanparentmaterials.Jointbend'sstrengthsareenhancedduetothehighermetal-to-metaljunctionproducinganon-planarbondlines.Nevertheless,thetraditionaltransientliquidphasediffusionbondingproducesplanarones.Bondingparametersofnewprocessare1260℃for0.5minand1230℃for4min.
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简介:AhighsensitivityD-shapedholedouble-claddingfibertemperaturesensorbasedonsurfaceplasmonresonance(SPR)isdesignedandinvestigatedbyafull-vectorfiniteelementmethod.WithintheD-shapedholedoublecladdingfiber,thehollowD-sectioniscoatedwithgoldfilmandtheninjectedinahighthermo-opticcoefficientliquidtorealizethehightemperaturesensitivityforthefiberSPRtemperaturesensor.ThenumericalsimulationresultsshowthatthepeakinglossoftheD-shapedholedouble-claddingfiberSPRishugelyinfluencedbythedistancebetweentheD-shapedholeandfibercoreandbythethicknessofthegoldfilm,butthetemperaturesensitivityisalmostinsensitivetotheaboveparameters.Whenthethermo-opticcoefficientis-2.8×10-4∕℃,thethicknessofthegoldfilmis47nm,andthedistancebetweentheD-shapedholeandfibercoreis5μm,thetemperaturesensitivityoftheD-shapedholefiberSPRsensorcanreachto-3.635nm∕℃.
简介:Microstructureoftransientliquidphase(TLP)diffusionbondedathirdgenerationsinglecrystalsuperalloyjointwasinvestigatedusingscanningelectronmicroscopy(SEM),andmechanicalpropertiestestofjointwascarriedout,forobtainingrelationshipbetweenmicrostructureandmechanicalpropertiesofjoint.Theresultsshowedthatthejointcontainedbondingzoneandbasemetal.Thediffusionzonewasobviouslyobserved.Whenitwasnotfinishedforisothermalsolidificationprocess,thebondingzonewouldcontainisothermalsolidificationzoneandrapidsolidificationzone.Metallographicexaminationrevealedthatisothermalsolidificationzonewasconsistedofyandphase.Rapidsolidificationzonewasconsistedoftwodifferentstructures,whichwereternaryeutecticofborides,yandy,phasedevelopingattheedgeofjoint,binaryeutecticofyandphaseappearingintheportionofjoint.Whenitwasnotenoughforhomogenizationprocessundertheconditionoffinishingisothermalsolidificationprocess,thebondingzonewouldcontainisothermalsolidificationzoneandboridesattheinterface.Undertheconditionsofrelativelyhighweldingtemperatureandlongweldingtime,averagetensilestrengthofjointwasequivalenttothatofparentmaterial.
简介:Neutronusuallyappearswithgamma,whichisrequiringthedetectorhasthecapabilityofngammadiscrimination.Pulseshapediscrimination(PSD)isacommonapproachofn,gammajudgment,butrequiredacomplexprocesstoselectasuitablediscriminationfactor,andpoorperformanceinthelowenergyrange.AmethodbasedonthetimeintervalofadjacentSignalswasdisruptedandadoptedtocomparetopulseshapediscriminationinthefastneutrondetectionmethod.AgoodagreementbetweentheadoptedmethodandPSDmethodwasachieved,includingthetotalcountratioandneutroncountratio.Thecomparisonprovesthecorrectnessofthetheoreticalderivationandvalidatesthemethodinpractice.TheadvantagesandlimitationsofthemethodbasedontimeIntervalofadjacentsignalswereanalyzed.Themethodprovidesaneffectivewaytoconfirmthecalibrationoftheneutrondetectionofaliquidscintillationdetector.Also,asasimplewayonlyrequiringthetimeinformationaboutevents,thedescribedmethodhaslargeapplicationpotentialinsomecaseoffastneutronfluxorintensitymeasurement.
简介:这研究向动人的表面为三维的麦克斯韦液体集中于热和集体流动的Cattaneo-Christov理论。有可变热电导率的不可压缩的laminar流动被考虑。流动产生由于表的双向拉长。热和集体运输的联合现象被说明。热和集体散开的Cattaneo-Christov模型被用来开发精力和集体种类的表情。在集体种类方程的一阶的化学反应术语被考虑。边界层假设导致管理数学模型。homotopic模拟被采用设想无尺寸的流动方程的结果。速度,温度,和集中的图显示出不同产生参数的效果。一个数字基准被介绍设想计算结果的会聚的价值。结果证明集中和温度地为热和集体散开的Cattaneo-Christov理论被腐烂。
简介:Inthiswork,acidfunctionalizedmulti-wallcarbonnanotubes(MWCNTs)weremodifiedwithimidazolium-basedionicliquids.Theselectiveoxidationofvariousalcoholswithhydrogenperoxidecatalyzedby[PZnMo_2W_9O_(39)]~(5-),ZnPOM,supportedonionicliquids-modifiedwithMWCNTs,MWCNTAPIB,isreported.Thiscatalyst[ZnPOM@APIB-MWCNT],wascharacterizedbyX-raydiffraction,scanningelectronmicroscopy(SEM)andFT-IRspectroscopicmethods.Thisheterogeneouscatalystexhibitedhighstabilityandreusabilityintheoxidationreactionwithoutlossofitscatalyticperformance.
简介:Si-Miao-Wan(SMW),atradiationalChinesemedicinalformulaconsistingofAtractylodisRhizoma,PhellodendriChinensisCortex,CoicisSemen,andAchyranthisBidentataeRadix,hasbeenusedforthetreatmentofgoutandgoutyarthritisformanyyears.Inthepresentstudy,aliquidchromatographyquadrupole-time-of-flightmassspectrometry(LC-Q-TOF/MS)methodwasestablishedtoidentifythemultipleconstituentsofSMWanditsmetabolitesinratbiologicalsamplesafteroraladministration.Atotalof48compoundsinSMW,including21alkaloids,12organicacids,2terpenes,3lactones,2phytosterols,and8othercompounds,weretentativelycharacterizedwiththediagnostic-ionfilteringstrategy.BasedonthediagnosticionsappliedtoidentifycompoundsinSMW,28prototypecompoundsand10metaboliccompoundsweredetectedinthebiologicalsamples.ThiswasthefirstcomprehensivedrugmetabolisminvestigationofSMWinrats.Thedevelopedmethodcouldbeausefulmeansforidentifyingthemulti-componentsinSMWandthemetaboliccomponents.TheresultsmayhelpexplorethepossiblemetabolicprocessesandmechanismofactionforSMWinvivo.