简介：ThedosimetricphosphorsLi_3PO_4:M(M=Tb,Cu)wereproducedbymodifiedsolid-statemethod.ThestructuralandmorphologicalcharacterizationwascarriedoutthroughX-raydiffraction(XRD)andscanningelectronmicroscope(SEM).Additionally,thephotoluminescence(PL),thermoluminescence(TL)andopticallystimulatedluminescence(OSL)propertiesofpowderLi_3PO_4dopedwithTbandCuwerestudied.ItisadvocatedthatLi_3PO_4:CuphosphornotonlyshowshigherOSLsensitivity(25timesormore)butalsogivesfasterdecayinOSLsignalsthanthatofLi_3PO_4:Tb~(3+)phosphor.Theminimumdetectabledose(MDD)ofLi_3PO_4:M(M=Tb,Cu)phosphorsisfoundtobe21.69×10~(-3)and3.33×10~(-6)J·kg~(-1),respectively.InOSLmode,phosphorshowslineardoseresponseintherangeof0.02-20.00J·kg~(-1).InTLmode,sensitivityofLi_3PO_4:CuphosphorismorethanthatofLi_3PO_4:Tbphosphor.Thekineticsparameterssuchasactivationenergyandfrequencyfactorsweredeterminedbypeakshapemethod,andphotoionizationcrosssectionsofpreparedphosphorwerecalculated.

简介：FluorescenceandcofluorescencepropertiesofTb(Ⅲ)solidcomplexeswerestudiedusingpyromelliticacid(PMA)asligandandfluorescenceinertionsasdopingelements.Thecofluorescenceenhancement,aresultofligandsensitizedfluorescence,wasobservedinTb(Ⅲ)solidcomplexesdopedwithfluorescentinertionsLa(Ⅲ),Gd(Ⅲ),Ca(Ⅲ),andSr(Ⅲ).Theeffectofthetypeandcontentofdopingelementsonfluorescenceenhancementwasstudied,andoptimumconditionsweredetermined.TheresultsshowthatGd(La,Ca,Sr)hasclearcofluorescenceeffectinsolidcomplexTb-M-PMAsystem,andinpresentwork,rareearthcomplexfluorescentpowderthatemitsbrightgreenfluorescenceatultravioletexcitationwasobtained,whichhadpotentialapplicationasfluorescentanti-counterfeitink.

简介：利用扫描电子显微镜、能谱仪、光学金相显微镜、光谱仪等仪器,对40Mn2锻造磨球以及锻造坯料进行组织分析和化学成分测定,探讨了生产过程中锻造磨球出现裂纹和心部孔洞等缺陷的主要原因。结果表明：锻造坯料中存在较严重的带状组织和缩孔、夹杂等缺陷;同时锻造磨球淬火过程中热处理工艺参数不合理,形成粗大的魏氏组织;建议在冶炼过程中添加去渣剂,在轧制生产过程后增加均匀化退火处理,在锻造生产中调整加热、冷却条件以避开魏氏组织生成区域。

简介：Basedonclustervariationmethod(CVM)andnaturaliterationmethod(NIM),order-disorderphasetransitionintheintercalationcompoundsM1/2TiS2issimulatedbycomputer.Thefavorableconditions,underwhich3a0×a0superstructureisformed,aregiven,andtheresultsareingoodagreementwiththeexperimentsandtheoreticalcalculations.TherelationshipbetweencriticaltemperatureandM-ion-vacancyinteractionparameterislinear.

简介：InordertoimprovetheelectrochemicalcyclestabilityofLa-Mg-Nisystem(PuNi3-type)hydrogenstoragealloy,NiinthealloyswaspartiallysubstitutedbyM(M=Cu,Al,Mn).AnewLa-Mg-NisystemelectrodealloysLa0.7Mg0.3Ni2.55-xCo0.45Mx(M=Cu,Al,Mn;x=0,0.1)werepreparedbycastingandrapidquenching.Theeffectsofelementsubstitutionandrapidquenchingonthemicrostructuresandelectrochemicalperformancesofthealloyswereinvestigated.TheresultsbyXRD,SEMandTEMshowthatthealloyshaveamultiphasestructure,includingthe(La,Mg)Ni3phase,theLaNi5phaseandtheLaNi2phase.Therapidquenchingandelementsubstitutionhaveanimperceptibleinfluenceonthephasecompositionsofthealloys,butbothchangethephaseabundanceofthealloys.Therapidquenchingsignificantlyimprovesthecompositionhomogeneityofthealloysandmarkedlydecreasesthegrainsizeofthealloys.TheCusubstitutionpromotestheformationofanamorphousphaseintheas-quenchedalloy,andareversalresultbytheAlsubstitution.Theelectrochemicalmeasurementindicatesthattheelementsubstitutiondecreasesthedischargecapacityofthealloys,whereasitobviouslyimprovesthecyclestabilityofthealloys.ThepositiveinfluenceofelementsubstitutiononthecyclelifeofthealloysisinsequenceAl＞Cu＞Mn,andnegativeinfluenceonthedischargecapacityisinsequenceAl＞Mn＞Cu.Therapidquenchingsignificantlyenhancesthecyclestabilityofthealloys,butitleadstoadifferentextentdecreaseofthedischargecapacityofthealloys.

简介：对多次电镀铬的300M钢试样的疲劳性能、氢脆倾向、疲劳断口进行了测试和分析，以研究镀铬次数、镀铬层厚度对300M钢疲劳性能的影响规律。结果表明：镀铬层对300M钢的疲劳性能影响很大，在试验条件下，带镀层试样较未电镀试样的疲劳强度和相同应力条件下的疲劳寿命降低约60％，且镀层越厚疲劳寿命越低；这种影响与电镀次数无明显关系，只要执行正常的除氢工艺，重复电镀多达15次的300M钢仍未发现氢脆倾向。断口分析表明：疲劳裂纹主要起源于镀铬层或镀层与基体的界面处，疲劳性能的大幅降低主要与镀铬层本身的特性有关。

简介：掌握润滑油中磨粒的尺寸和浓度信息可以获知设备的润滑状态，从而可以采取针对性的维护措施，预防设备过早失效。本研究以自制的在线润滑油磨粒检测传感器为平台，将油液中铁磁性磨粒经过时产生的电磁扰动转换为相对应的电压信号，并设计硬件电路将此电压信号转化成真有效值信号；同时提出一种基于局部加权回归的平滑滤波算法（LOWESS）对信号进行降噪和特征提取，以在温漂、零漂、电磁干扰等噪声环境下实时获取润滑油中磨粒的尺寸和浓度信息；最后将检测结果与MetalSCAN3110磨粒传感器的结果对比，证明了该方法的可行性。

简介：超华科技（002288）2月20日晚间公告，根据《广东省著名商标认定和管理规定》和《广东省工商行政管理局关于广东省著名商标认定和管理的实施细则》的规定，经广东省著名商标评审委员会评审通过，公司“M”商标被延续认定为“广东省著名商标”，认定商品为“覆铜箔层压酚醛树脂板（绝缘材料）”，有效期自2013年3月24日起至2016年3月23日止。

简介：本文对比分析了氮基保护气氛和真空两种热处理加热介质对300M钢疲劳性能的影响，并研究了热处理后表面喷丸强化对300M钢疲劳性能的改善情况。结果表明，由于氮基保护气氛热处理后表面层有一定程度的氧化脱碳，故钢的疲劳极限比真空热处理的低近30％；由于喷丸强化后表面形成较大的压应力，消除了表面氧化层等不良影响，氮基保护气氛热处理后经喷丸的300M钢疲劳极限比未喷丸的提高约40％。