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  • 简介:Inthispaper,weproposeandexperimentallydemonstrateamethodtorealizeapolarizationdetectorbyusingacommerciallyavailablepolymethylmethacrylate(PMMA)pipe.Anasymmetricpolarization-relatedstructureisfabricatedbyetchingdifferentgratingstructuresontheexternalsurfaceofthepipe.Theresultsshowthatwhenthepiperotatesupto90°,thepeakofthetransmissionspectrumcanevidentlyshifttowardsthelowfrequency,whichmeansthepipewithgratingstructurescanserveasapolarizationdetector.Thisdesignpossessesthemeritsofasimplestructureandeasyfabrication.

  • 标签: 偏振相关 探测器 太赫兹 玻璃管 聚甲基丙烯酸甲酯 光栅结构
  • 简介:WedemonstratethegenerationofQ-switchedpulsesfromanytterbium-dopedfiberlaser(YDFL)usingquantumdot(QD)CdSeasapassivesaturableabsorber(SA).TheCdSeQDisfabricatedbythesynthesisofCdO,Se,andmanganeseacetateandparaffinoilandoleicacidasthesolventandsurfactant,respectively.TheCdSeQDisthendopedintopoly-methyl-methacrylate(PMMA)viaanemulsionpolymerizationprocess.APMMAhostedCdSeQDthinflakewithahomogeneousendsurfaceisthenformedandplacedbetweentwoferrulesandassembledinaYDFLcavitytoachievetheQ-switchingoperationwitharepetitionrateof24.45to40.50kHzwhilevaryingthepumppowerfrom975to1196mW.Thepulsewidthchangesfrom6.78to3.65μswithamaximumcalculatedpulseenergyat0.77μJatapumppowerof1101mW.ThisworkmaybethefirstdemonstrationofCdSeQD-basedQ-switchinginanall-fiberconfigurationthatshouldgiveproportionalinsightintosemiconductorQDmaterialsinphotonicsapplications.

  • 标签: CdSe量子点 可饱和吸收体 全光纤结构 调Q脉冲 PMMA 激光掺杂
  • 简介:目的分析直入式骨水泥注入椎体强化方法在体外提高螺钉稳定性的效果。方法采用新鲜尸体脊柱标本共24个椎体,一侧椎弓根采用直入式注入PMMA骨水泥强化椎弓根钉固定作(试验组),另一侧椎弓根采用常规椎弓根螺钉固定(对照组),两侧进行最大轴向拔出力试验、最大旋出力矩试验、周期抗屈试验生物力学测试,比较两组测试结果。结果骨水泥强化组中螺钉的稳定性均显著强于单纯常规椎弓根螺钉组(P〈0.05)。结论应用PMMA行椎体强化椎弓根钉固定有利于增强对椎弓根钉的把持力,可有效防止椎弓根钉的松动及脱落,具有良好的临床效果。

  • 标签: 骨水泥强化 椎弓根钉 生物力学
  • 简介:ThisarticleaddressesthesynthesisoforganicallytailoredNi-Allayereddoublehydroxide(ONi-AlLDH)anditsuseinthefabricationofexfoliatedpoly(methylmethacrylate)(PMMA)nanocomposites.ThepristineNi-AlLDHwasinitiallysynthesizedbyco-precipitationmethodandsubsequentlymodifiedusingsodiumdodecylsulfatetoobtainONi-AlLDH.NanocompositesofPMMAcontainingvariousamountsofmodifiedNi-AlLDH(3wt%?7wt%)weresynthesizedviasolventblendingmethodtoinvestigatetheinfluenceofLDHcontentonthepropertiesofPMMAmatrix.SeveralcharacterizationmethodssuchasX-raydiffraction(XRD),transmissionelectronmicroscopy(TEM),Fouriertransforminfraredspectroscopy(FTIR),rheologicalanalysis,differentialscanningcalorimetry(DSC)andthermogravimetricanalysis(TGA),wereemployedtoexaminethestructural,viscoelasticandthermalpropertiesofPMMA/OLDHnanocomposites.TheresultsofXRDandTEMexaminationconfirmtheformationofpartiallyexfoliatedPMMA/OLDHnanocomposites.TheFTIRresultselucidatethatthecharacteristicbandsforbothpurePMMAandmodifiedLDHarepresentinthespectraofPMMA/OLDHnanocomposites.Rheologicalanalyseswerecarriedouttoexaminetheadhesionbetweenpolymermatrixandfillerspresentinthenanocompositesample.TheTGAdataindicatethatthePMMAnanocompositesexhibithigherthermalstabilitywhencomparedtopurePMMA.ThethermaldecompositiontemperatureofPMMA/OLDHnanocompositesincreasesby28KcomparedtothatofpurePMMAat15%weightlossasapointofreference.IncomparisonwithpurePMMA,thePMMAnanocompositecontaining7wt%LDHdemonstratesimprovedglasstransitiontemperature(Tg)ofaround3K.Theactivationenergy(Ea),reactionorders(n)andreactionmechanismofthermaldegradationofPMMA/OLDHnanocompositeswereevaluatedusingdifferentkineticmodels.WateruptakecapacityofthePMMA/OLDHnanocompositesislessthanthatofthepurePMMA.

  • 标签: 聚合物/纳米复合材料 PMMA 溶液共混法 LDH 热性能 合成