简介:ThemicrostructuralchangesofFe83Si4B13amorphousmotheralloyduringtheheatingprocesswereinvestigatedbyLaserScanningConfocalMicroscopy(LSCM),andthephasetransformationwasdeterminedbytheThermo-Calccalculations.ThedifferencesinthemeltingpointsmeasuredbyDifferentialScanningCalorimetry(DSC)andLSCM,andthoseobtainedbyThermo-Calccalculationswerealsodiscussed.ItisfoundthatthemeltingpointsmeasuredbyDSCandLSCMarerelativelysimilar,whereastheonsetandendofthemeltingtemperaturescalculatedbyThermo-CalcsoftwarearehigherthanthosemeasuredbyDSCandobservedbyLSCM.
简介:采用单辊法制备了宽20mm、厚25μm的Fe78Si9B13合金带材,用绕带机将其绕制成环型磁芯,然后将磁芯进行退火处理,结果表明,随着退火温度的升高,Fe78Si9B13非晶磁芯的初始磁导率m、饱磁感应强度Bs和矫顽力Hc呈先增大后减小的趋势,当退火温度达到450℃时,磁化曲线呈现出一定的线性关系,即恒导磁特性。将经4500(=/100min退火的Fe78Si9B13非晶磁芯用环氧树脂进行封装后,环氧封装后μi和Bs减小,而Hc和损耗Ps增大,磁化曲线和损耗曲线的形状与封装前相同。
简介:铁矿石经浓盐酸和少量的SnCl2溶液加热到45℃溶解后,用SnCl2-TiCl3还原滴定Fe(Ⅲ),使Fe(Ⅲ)还原为Fe(Ⅱ),再以K2Cr2O7滴定全铁含量。本方法对实验操作温度,试样溶解酸的选择有一定的要求,宜选用非氧化性强酸在30-60℃溶解矿样。
简介:Toeffectivelysolvetheagglomerationproblemsinthesolidstatereactionprocess,pre-addingglucoseisadoptedtothesynthesisofLiFePO4/CenergymaterialsusingFe–Pwasteslag.Theaverageparticle&grainsizeofLiFePO4/Cdecreases,andtheimpuritiesinLiFePO4/Ccompositesreducetoagreatextent.Itmakesgreatsensetothemassindustrialproduction.Theoptimumsynthesisconditionsdeterminedinthisworkarebasedontheorthogonalexperiments.Thesamplessynthesizedinascaleof500gexhibithighpurity,excellentelectrochemicalperformance,highreactionactivity,goodreversibility,andlowpolarizationlevel.Thedischargecapacitiesare145,134,117,and102mAh/gatthecurrentdensitiesof0.1C,0.2C,0.5Cand1C,respectively.ThisworkputsforwardapracticalsuggestionformassproducingenvironmentalbenignandlowcostLiFePO4/Cascathodematerialsoflithiumionbatteries.
简介:Intrinsiccarrierconcentration(ni)isoneofthemostimportantphysicalparametersforunderstandingthephysicsofstrainedSiandSi1-xGexmaterialsaswellasforevaluatingtheelectricalpropertiesofSi-basedstraineddevices.Uptonow,thereportonquantitativeresultsofintrinsiccarrierconcentrationinstrainedSiandSi1-xGexmaterialshasbeenstilllacking.Inthispaper,byanalyzingthebandstructureofstrainedSiandSi1-xGexmaterials,boththeeffectivedensitiesofthestatenearthetopofvalencebandandthebottomofconductionband(NcandNv)at218,330and393KandtheintrinsiccarrierconcentrationrelatedtoGefraction(x)at300KweresystematicallystudiedwithintheframeworkofKPtheoryandsemiconductorphysics.ItisfoundthattheintrinsiccarrierconcentrationinstrainedSi(001)andSi1-xGex(001)and(101)materialsat300KincreasessignificantlywithincreasingGefraction(x),whichprovidesvaluablereferencestounderstandtheSibasedstraineddevicephysicsanddesign.
简介:Moleculardynamics(MD)simulationswereperformedtostretchtherectangulargraphenesheetsdopedwithsilicon,nitrogenorboronatoms.Young’smodulus,ultimatestress(strain)andenergyabsorptionweremeasuredforthegraphenesheetswiththedopingconcentration(DC)rangingfrom0to5%.Theemphasiswasplacedonthedistincteffectsofeachindividualdopantonthefundamentalmechanicalpropertiesofgraphene.TheresultsindicatedthatincorporatingthedopantsintographeneledtoanalmostlineardecreaseinYoung’smodulus.Monotonicreductionsinultimatestrength,ultimatestrainandenergyabsorptionwerealsoobserved.Suchdopingeffectswerefoundtobemostsignificantforsilicon,lesspronouncedforboron,andsmallornegligiblefornitrogen.Theoutputsprovideanimportantguidanceforthedevelopmentandoptimizationofnovelnanoscaledevices,andfacilitatethedevelopmentofgraphene-basedM/NEMS.
简介:SiC/Si<潜水艇class=“a-plus-plus”>3N<潜水艇class=“a-plus-plus”>4合成是用自我繁殖的高温度的燃烧合成-Si3N<潜水艇class=“a-plus-plus”>4粉末和适当数量原文如此搽粉。两个都,sintering添加剂,系统被使用,它是YAN(Y2O3艾尔2O3AlN)并且YN(Y2O3AlN)。影响在SiC/Si的sintering行为上原文如此满意<潜水艇class=“a-plus-plus”>3N<潜水艇class=“a-plus-plus”>4合成被调查。结果证明有二个sintering添加剂系统的样品的密度,收缩,弯曲力量,坚硬,和破裂坚韧随内容的增加增加第一原文如此然后甚至当原文如此内容不断地增加时,减少。样品的重量损失的趋势是相反的。有最好的机械性质的样品原文如此满意在二个系统是不同的。为YAN系统,当原文如此内容到达10时,样品的最好的机械性质被获得?%,当至于YN系统它是5时?%。YN样品的性质比YAN样品优异。J阶段(2Y2O3吠敨爠畯整漠?灡汰楹杮氠睯瀠敲獳牵?景???慐漠?桴?獡搭獩牰灯牯楴湯瑡摥朠敲湥挠浯慰瑣搠牵湩?桴?敤潳灲楴湯爠'啼礃A慮楴湯瀠潲散獳椠?楳畴栠瑯搠晥牯慭楴湯椠??灳牡?汰獡慭猠湩整楲杮?偓?猠獹整?慣?扯慴湩挠浯汰瑥汥?敲潣扭湩摥丠??洠条敮?楷桴朠潯?湡獩瑯潲祰愠摮洠条敮楴?牰灯牥楴獥?桔?慭楸畭?慭湧瑥捩瀠潲数瑲敩??????汣獡?愢瀭畬?汰獵?慭?猯'T?????鮪徬鞪??极脿???醰鑛??鴿鎘銳????�
简介:Thisstudyaimstoinvestigatetheeffectofthe1-stepquenchingandpartitioning(Q&P)processonthemicrostructureandtheresultingVicker’shardnessof0.3C-1.5Si-1.5Mnsteelbyusingin-situdilatometry,opticalmicroscopy(OM),scanningelectronmicroscopy(SEM),X-raydiffractometry(XRD),andVicker’shardnessmeasurement.Systematicanalysesindicatethatthemicrostructureofthespecimensquenchedandpartitionedat150℃,200℃,250℃,and300℃mainlycompriseslathmartensiteandretainedaustenite.Thedilatometrycurveofthespecimenpartitionedat150℃ispresumablyascribedtotheformationofisothermalmartensite.Intheearlystagesofpartitioningat200℃,thenearlyunchangeddilatationcurveiscloselyrelatedtothesynergisticeffectofisothermalmartensiteformationandtransitionalepsiloncarbideprecipitation.Inthelaterstagesofpartitioningat200℃,theslightincreaseinthedilatationcurveisduetothecontinuousisothermalmartensiteformation.Withfurtherincreaseinpartitioningtemperatureto250℃,thedilatationincreasesgraduallyupto3600s,whichisrelatedtocarbonpartitioningandlowerbainiteformation.Partitioningatahighertemperatureof300℃causesarapidincreaseinthedilatationcurveduringtheinitialstages,whichsubsequentlylevelsoffuponprolongingthepartitioningtime.Thisismainlyattributedtotherapiddiffusionofcarbonfromathermalmartensitetoretainedausteniteandcontinuousformationoflowerbainite.
简介:采用溶胶-凝胶法制备了Mn离子摩尔掺杂比.32分别为0,2%,4%,6%,8%的Ba(Ti1-xMnx)O3铁电薄膜。研究发现:当x为6%时,漏电流和矫顽场均达到最小,与未掺杂时相比,漏电流降低了约3个量级,矫顽场电场强度降低了约60%,P—E回线的矩形度增加。实验结果表明:通过适量掺杂Mn离子,可以改善BaTiO3铁电薄膜电学性能,提高铁电薄膜的极化,降低薄膜的漏电流。
简介:Theneutron-richisotopeswithN40below68Ni,inmanywaysbehavesimilartothe“islandofinversion”nucleiwithN20.Wereportonthemeasurementsofexcitedstatesof63;65;67Mnviain-beam-rayspectroscopy.TheexperimentwasperformedattheRadioactiveIsotopeBeamFactory,RIKEN.Analysisofdatafor63;65;67MnobtainedintheSEASTARcampaignhasbeendone.Afewtransitionshavebeenidentifiedineachofthemprovidingachancetostudythesystematicstructureevolutionofn-richMnisotopesnearN40.
简介:TheresistivityofHg0.89Mn0.11Tehasbeenmeasuredbythesuperconductingquantuminterferencedevicemagnetometerinthetemperaturerangefrom5to200Kundertheappliedmagneticfieldof1,2,4and6.5Tesla,respectively,comparedwiththatofno-magneticfield.Theresultsshowthattheresistivityincreaseswithincreaseappliedmagneticfieldathighertemperaturefrom80to200K,butdecreasesatlowertemperaturefrom5to25K.Thereexistsatransitiverangefrom25to80K,wherethevariationoftheresistivityshowsdifferenttendenciesdependingonthestrengthofmagneticfield.Maximumdifferenceofresistivityunder6.5Teslafromthatwithoutmagneticfieldinthetemperaturerangefrom30to200Kisonlyabout5Ω·cm,butitincreasesupto3ordersofmagnitudeat5K.TheanalysisshowsthatthevariationofresistivityofHg0.89Mn0.11Teunderthemagneticfieldisthealgebraicsumofthetransversedirectionmagnetoresistanceeffectandthesp-dexchangeinteractioneffect.TDRMEplaysmajorroleinthehightemperaturerange.However,withthedecreaseoftemperature,theeffectofsp-dEIontheresistivitygraduallyexceedsthatofthetransversedirectionmagnetoresistanceeffectthroughthetransitiverange,andbecomesthedominanteffectinthetemperaturerangefrom5to25K,whichleadstothedramaticdecreaseofresistivity.
简介:通过EMS(Ethylmethylsulfonate,甲基磺酸乙酯)诱变豫谷1号获得一个遗传稳定的谷子小穗突变体si-sp1,该突变体突出表现为穗部变小,同时伴随有株高降低、单码小花数减少和根系变小等表现型变异。与野生型豫谷1号相比,突变体的穗长和株高分别降低了37.8%和9.0%,单穗粒重和单码小花数分别降低了40.3%和31.7%,但千粒重增加了20.2%。遗传分析表明,si-sp1突变性状由1对隐性基因控制。以si-sp1为母本、辽谷1号为父本构建的F2定位群体的隐性单株,将突变基因定位在8号染色体上CAAS8003与SSR1038间约11.02M的距离内,为下一步精细定位并分离该基因奠定了基础。
简介:判断液压设备故障要求具备相应的专业知识,通晓单体设备的工作方式及其在整个控制系统中的功能,尤其是电气和液压线路图。根据维修西马克挤压机液压系统故障的工作经验,以最具代表性的18MN西马克挤压机为研究对象,重点分析18MN西马克挤压机挤压力故障产生的原因及其处理方法。
简介:在同一直线上的双脉搏的导致激光的故障光谱学被使用一双毫微秒Nd在Si水晶上执行:在1064nm射出的钇铝柘榴石激光来源。光谱紧张和选择Si原子、离子的线的signalto-噪音比率被用来评估光排放。当改变interpulse延期时间和二的精力比率时,光排放紧张被记录搏动的激光。线紧张和signal-to-noise比率上的数据获得延期时间的效果也被调查了。基于结果,最佳的interpulse延期时间,二的精力比率搏动了激光,和完成原子、离子的最大值的数据获得延期时间衬里紧张被作出对有利的裁决有在同一直线上的双脉搏的激光途径的Si血浆的产生。为观察的线紧张变化的主导的机制也被讨论。另外,在不同的门的血浆温度和电子数字密度推迟时间和不同interpulse延期时间被导出。血浆在更短的interpulse延期时间在电子温度和电子数字密度上防护的重要影响被观察。